ReviewModeling of preparative liquid chromatography
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2019, Separation and Purification TechnologyAdsorption behavior of optical brightening agent on microfibrillated cellulose studied through inverse liquid chromatography: The need to correct for axial dispersion effect
2018, Journal of Chromatography ACitation Excerpt :This method allowed characterizing the competitive adsorption between the enantiomers. Axial dispersion affects the shape of breakthrough curves, thus impacts the identification of adsorption isotherm parameters [34]. Heater and Liapis, studied the effect of axial dispersion on the efficiency of adsorption process, through modelling.
Evolution and status of preparative gas chromatography as a green sample-preparation technique
2015, TrAC - Trends in Analytical ChemistryCitation Excerpt :However, chromatography on capillary columns is generally characterized by higher speed and resolution, but, as mentioned above, lower sample capacity, which is the crucial point in prep-GC. The optimization of one separation parameter affects the others increasing mobile phase flow rate in order to reduce the collection time results in a decrease in efficiency and, as a consequence, in resolution, which is also impaired if column overloading arises from an excessive sample volume or excessive sample mass [12]. The sample capacity depends in turn on certain variables, such as column internal diameter (ID), length and film thickness (f.t.).
Facile optimization for chromatographic separation of liquiritin and liquiritigenin
2013, Journal of Chromatography ACitation Excerpt :For a mixture such as natural product with multiple unknown components, it is impossible to obtain the accurate adsorption isotherms and chromatographic models. A considerable simplification of the model with negligible loss of accuracy can be achieved by making some simple assumptions [14]. Flavonoid is one kind of the active components in licorice.
Effect on separation of injecting samples in a solvent different from the mobile phase
2007, Journal of Chromatography A